This thesis presents a comprehensive approach to designing an experimental procedure for the validation of an electro-adhesive technology produced through printed electronic in a space-like environment: a thermal vacuum chamber testing campaign. This electro-adhesive technology is designed to be used in space missions for active debris removal and in-orbit servicing. Current space operations involving grasping and handling of asset are limites by establishing a physical interface with objects in a hostile environment such as space. The objective of this project is to demonstrate that an electro-adhesive technology is suitable for space applications concerning thermovacuum conditions. This work was conducted at AdapTronics, a deep tech start-up that produces adaptive mechatronic devices.